X-Ray Diffraction

X-Ray diffractometric techniques can be applied to investigate a variety of material properties. Powder/bulk analyses include phase identification and quantification as well as atomic structure determinations. Thin film/surface investigations include residual stress, texture (crystallographic orientation), and reflectometry for atomic scale roughness and void density determinations.

Three individually unique Philips goniometric systems, on two separate generators, allow automated loading and programming of 68 separate samples for unattended 24/7 data acquisition.

System Capabilities:
» Phase identification referenced to a licensed annually updated international database of > 131,000 phases
» Advanced software data manipulation, including several Rietveld packages, atomic modeling, full profile fit, simulation, stress, texture, and more
» Crystallite size, lattice constants, micro strain, residual stress, reflectometry
» Cu k-alpha standard radiation source (additional sources available)
» 100µm focal spot size monocapillary collimator (small spot analysis on inhomogeneous samples)
» Spinning micro diffraction stage (small powder quantities mounted in a glass capillary)
» Diffracted beam monochromators and sample spinners
» Phi and Psi rotation open Eularian cradle with z-translation and wafer (to 100 mm) stage (stress, rocking curves, texture, reciprocal space mapping)
» Polycapillary incident lens with diffracted beam collimator/flat monochromator for parallel beam geometry
» High resolution rocking curve analysis, reciprocal space mapping and X-ray topography of epitaxial layers on single crystal substrates
» Incident monochromatic radiation with hybrid mirror/2-crystal bounce optic
» Transmission measurements through thin foils


XRD X'Pert Pro Diffractometer System



XRD Dual Diffractometer System

 

Ovonic sm

 

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